Abstract
Friction stir processing (FSP) is a new solid-state processing technique for microstructural modification based on friction stir welding (FSW) developed by The Welding Institute (TWI) in 1991. Since its invention, the process has continually been improved, and its scope of application expanded leading to industrial applications and commercialisation in the microstructural modifications of materials to achieve desired mechanical properties. The literature review investigates studies already conducted in the field of FSP on different aluminium materials. However, no published work on the correlation of microstructural homogeneity in multi-friction processed zone with mechanical properties seem to exist despite the fact that inhomogeneity in the friction processed zone might be a reason for the degradation in mechanical properties of single-pass FSP processed materials. This dissertation focuses on the effect of multi-pass FSP on aluminium. FSP was conducted using constant rotational and transverse speeds of 1600 rpm and 40 mm/min respectively. A tool plunge depth of 5.3 mm and a 3° tilt angle was used. AA6061-T6 was the selected matrix alloy, and its microstructural homogeneity in correlation with the evolving mechanical properties after each successive FSP pass was studied in detail. Macrostructural and microstructural characterisation was carried out with an optical microscope (OM) and a scanning electron microscope (SEM), while tensile testing, and microhardness profiling was carried out to evaluate the mechanical properties of the processed materials using a tensile testing machine and a Vickers microhardness tester respectively. A study of the underlying thermodynamics occurring during the FSP process was also conducted using molecular dynamics (MD) simulation. The macrostructural and microstructural evaluations of the processed samples revealed an increase in microstructural homogeneity as the number of FSP passes increases. The correlation of this homogeneity with the resulting mechanical properties indicates that a nearly 100% homogenous friction processed zone improved the mechanical properties in the processed aluminium materials. However, the BM was found to have better mechanical v properties with an ultimate tensile strength (UTS) of 338 MPa, a yield strength of 311 MPa, and an average Vickers microhardness of 99 HV, compared to the fully homogenous processed zone with a UTS of 177 MPa, yield strength of 172 MPa, and average Vickers microhardness of 67 HV. The resulting microstructural evolution and grain sizes after each FSP pass have also been observed to be strongly dependent on the processing parameters, thermal cycle, and presence of second-phase precipitates, rather than only on microstructural homogeneity. The results obtained from the MD simulation prove that it is possible to adequately represent MD simulations of FSP on aluminium alloys. The underlying thermodynamics was explained, and consistency between experimental FSP and the simulation process was achieved.
M.Eng. (Mechanical Engineering)